Pd K edge XAS fluorescence of 1 wt.% Pd/SiO2 at RT under H2 (after heating at 300C under H2)

Spectrum

Title: Pd K edge XAS fluorescence of 1 wt.% Pd/SiO2 at RT under H2 (after heating at 300C under H2)

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Data

Unit: Range: Valid spectral range(s): 195194228.827788 - 203283969.39695 eV

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References

DOI

10.26302/SSHADE/EXPERIMENT_SOC_20170316_001

Data reference

Ould-Chikh, Samy (2017): Pd K edge XAS fluorescence of 1 wt.% Pd/SiO2 at RT under He or H2 (after heating at 300C under H2). SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_SOC_20170316_001

Publications

Al-Shareef et al., 2018, J. Cat., 363, 34 - 51

Owner

Database

FAME

Experimentalists

Samy Ould-Chikh

Spectrum type

Experiment type: laboratory measurement
Type: fluorescence emission
Intensity unit: AU

Instrument #1

Instrument: X-ray Absorption Spectroscopy measured in fluorescence mode
Sample holder: FAME catalysis cell, see Aguilar-Tapia et al., Rev. Sci. Instrum., 2018

Spectral parameters

Standard medium

unknown

Observation mode

spectrum

Spectral range type(s)

hard X

Excitation wavelength

hard X

Valid spectral range(s)

	Min - Max ($eV$)	Sampling ($eV$)	Resolution ($eV$)	Position accuracy ($eV$)	Absorption edge
#1	24201.0 - 25204.0		1.25		$Pd$ (K: 24.3503 $keV$)

Comments

The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Pd metallic foil (first maximum of the derivative set at 24350 eV).