Experiment
Title
Pd K edge XAS fluorescence of 1 wt.% Pd/SiO2 at RT under He or H2 (after heating at 300C under H2)
DOI
10.26302/SSHADE/EXPERIMENT_SOC_20170316_001
Data reference
Ould-Chikh, Samy (2017): Pd K edge XAS fluorescence of 1 wt.% Pd/SiO2 at RT under He or H2 (after heating at 300C under H2). SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_SOC_20170316_001
Publications
Database(s)
Experimentalists
Type(s)
laboratory measurement
Number of spectra
3
Comments
These data were acquired on the BM30 beamline in the frame of the 30-02-1111 proposal.
Variable type(s)
  • other
Instrument
X-ray Absorption Spectroscopy measured in fluorescence mode
Sample holder
FAME catalysis cell, see Aguilar-Tapia et al., Rev. Sci. Instrum., 2018
Standard medium
unknown
Observation mode
spectrum
Spectral range type(s)
hard X
Valid spectral range(s)
Min - Max ($eV$) Sampling ($eV$) Resolution ($eV$) Position accuracy ($eV$) Absorption edge
#1 24200.99999999997 - 25204.000000000065 1.25 $Pd$ (K: 24.3503 $keV$)
Comments
The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Pd metallic foil (first maximum of the derivative set at 24350 eV).
Observation geometry
directional
Observation mode
fixed angles
Comments
Emitted x-rays are collected in a solid angle directed at 90 degrees from the incident beam.
Observation mode
single spot
Date begin - end
2017-03-16 - 2017-03-22

Versions

Release date
2021-07-20 12:05:32 UTC+0000
Version (Date)
#1 (2021-07-20 12:02:02 UTC+0000, Updated: 2021-07-20 12:05:32 UTC+0000)