Experiment
Title
Pt L3 edge XAS fluorescence and XAS transmission of Aqueous platinum chloride soutions at 600-700 nars and 30°C
DOI
10.26302/SSHADE/EXPERIMENT_GP_20180208_001
Data reference
Pokrovski, Gleb; Hazemann, Jean-Louis (2018): Pt L3 edge XAS fluorescence and XAS transmission of Aqueous platinum chloride soutions at 600-700 nars and 30°C. SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_GP_20180208_001
Type(s)
laboratory measurement
Description
Platinum (IV) and platinum (II) chloride aqueous solutions references at concentration around 0.1m Pt, in transmission and in fluorescence.
Number of spectra
6
Comments
These data were acquired on the BM30 beamline in the frame of the 30-02-1131 proposal.
Variable type(s)
  • sample composition
  • observation mode
Instrument
X-ray Absorption Spectroscopy measured in fluorescence mode
Sample holder
Institut Néel autoclave, see Testemale et al., Rev. Sci. Instrum., 2005.
Standard medium
unknown
Observation mode
spectrum
Spectral range type(s)
hard X
Valid spectral range(s)
Min - Max ($eV$) Sampling ($eV$) Resolution ($eV$) Position accuracy ($eV$) Absorption edge
#1 11446.9 - 12303.8 0.593 $Pt$ (L3: 11.5637 $keV$)
Comments
The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Pt metallic foil (first maximum of the derivative set at 11564 eV).
Observation geometry
directional
Observation mode
fixed angles
Comments
Emitted x-rays are collected in a solid angle directed at 90 degrees from the incident beam.
Observation mode
averaged
Instrument
X-ray Absorption Spectroscopy measured in transmission mode
Sample holder
Institut Néel autoclave, see Testemale et al., Rev. Sci. Instrum., 2005.
Standard medium
unknown
Observation mode
spectrum
Spectral range type(s)
hard X
Valid spectral range(s)
Min - Max ($eV$) Sampling ($eV$) Resolution ($eV$) Position accuracy ($eV$) Absorption edge
#1 11446.9 - 12303.8 0.593 $Pt$ (L3: 11.5637 $keV$)
Comments
The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Pt metallic foil (first maximum of the derivative set at 11564 eV).
Observation geometry
direct
Observation mode
fixed angles
Observation mode
averaged
Date begin - end
2018-02-08 - 2018-02-18

Versions

Release date
2022-12-13 11:19:20 UTC+0000
Version (Date)
#1 (2022-12-13 11:19:20 UTC+0000, Updated: 2022-12-13 11:19:20 UTC+0000)