Spectrum

Vis-NIR reflectance spectrum of Fontenaille pigment (PIG-0218-2019), sawn block

Title
Vis-NIR reflectance spectrum of Fontenaille pigment (PIG-0218-2019), sawn block
DOI
10.26302/SSHADE/EXPERIMENT_BS_20191012_100
Data reference
Schmitt, Bernard; Chalmin-Aljanabi, Emilie (2019): Vis-NIR reflectance spectra of Fontenaille pigments (PIG-0175-2016 + PIG-0218-2019): raw block, powders with different grain sizes and painted matter. SSHADE/PIG (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_BS_20191012_100
Experiment type
laboratory measurement
Type
reflectance factor
Comments
No photometry accuracy below 0.41 µm. Spectrum very noisy above 3.2 µm.
Instrument
SHADOWS Spectro-Gonio bidirectional reflection Vis-NIR
Sample holder
cylindrical aluminium sample holders of various sizes for powder
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
Vis
Valid spectral range(s)
Min - Max (nm) Sampling (nm) Resolution (nm) Position accuracy (nm) Absorption edge
#1 410.0 - 678.0 4.0 1.9 0.2
#2 682.0 - 802.0 4.0 3.8 0.4
Filters
Type Center/Edge (nm) Width (nm) Place
#1 several high frequency filters output of monochromator
Scan number
10
Comments
measured over the 362-802nm range, resolution slightly vary over the first grating: 1.94-1.90 nm
Observation geometry
bidirectional
Observation mode
fixed angles
Incidence angle
0.0°
Emergence angle
30.0°
Azimuth angle
0.0°
Phase angle
30.0°
Resolution illumination
5.8°
Resolution observation
4.1°
Illumination
Observation
Comments
some wavelength dependent polarization
Observation mode
single spot
Resolutions
5.2 ± 0.1 mm
Comments
illumination with 8 fiber optic spots within a 5.2 mm diameter, observation within an ellips of 23x20 mm
Instrument
SHINE Spectro-Gonio bidirectional reflection Vis-NIR
Sample holder
cylindrical aluminium sample holders of various sizes for powder
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
NIR
Valid spectral range(s)
Min - Max (nm) Sampling (nm) Resolution (nm) Position accuracy (nm) Absorption edge
#1 806.0 - 1426.0 4.0 3.8 0.4
#2 1430.0 - 3198.0 4.0 7.6 0.8
#3 3202.0 - 3234.0 8.0 15.5 1.6
Filters
Type Center/Edge (nm) Width (nm) Place
#1 several high frequency filters output of monochromator
Scan number
10
Comments
measured over the 402-4202nm range, resolutions slightly vary over the gratings: 3.88-3.77, 7.77-7.41, 15.52-15.42 nm. very noisy > 3234nm
Observation geometry
bidirectional
Observation mode
fixed angles
Incidence angle
0.0°
Emergence angle
30.0°
Azimuth angle
0.0°
Phase angle
30.0°
Resolution illumination
5.8°
Resolution observation
4.1°
Illumination
Observation
Comments
some wavelength dependent polarization
Observation mode
single spot
Resolutions
7.5 ± 0.2 mm
Comments
illumination with 9 fiber optic spots within 7.5 mm diameter, observation within an ellips of 23x20 mm
Experiment
Vis-NIR reflectance spectra of Fontenaille pigments (PIG-0175-2016 + PIG-0218-2019): raw block, powders with different grain sizes and painted matter
Date begin
2020-02-26
Release date
2020-06-25 12:04:48+0000 UTC
Version (Date)
#1 (2020-06-25 12:04:48+0000 UTC, Updated: 2022-11-07 07:49:38+0000 UTC)
History
Date Mode Version Status Comments
2020-06-25 11:20:31+0000 UTC first import #1 valid version
Analysis
raw bidirectional reflectance spectrum calibrated: 1) with "Spectralon 99%" measured under same geometry using its absolute BRDF (0.36-1.3µm) and 2) with "Infragold" using its relative spectral reflectance (1.3-4.2µm). The visible spectrum (0.36-0.8µm) is merged with the NIR spectrum (0.8-4.2µm). The residual water vapor lines, around 1.12, 1.38, 1.87, 2.665µm, have been corrected by multiplying by a scaled water vapor transmission spectrum measured at same resolution and sampling. A very slight smoothing (binomial over 3 points) has been applied, except in the narrow NIR absorption bands. A much stronger smoothing has been applied in the noisy part above 3.2µm (data acquisition problem with grating #4). The noisy flat 0.40-0.415µm part is strongly smoothed and extrapolated.
Quality flag
4
Validator(s)