Sample
Name
IOM from particle A0108_61
Date
2022-01-01
Provider
JAXA - remaining sample given back in June 2022
Parent sample
A0108_61
Substrate material
synthetic type IIa diamond windows
Substrate comments
between two 3 x 0.5 mm diamond windows
Temperature
22.0 2.0
Temperature max
22.0 2.0
Comments
IOM sample stored in dessicator under vacuum
Type
ambient air
Fluid temperature
22.0
Fluid pressure
1.0
Title
selection of the grains

Precursors

Matters

Produced sample

Materials
Processing steps
Step Chronology Date Type Process Changes
#1 before layer formation 2022-01-01 chemical Ultrapure water (Milli-Q water, 18.2 M) and CH3OH:CH3Cl (2/1 v/v) leaching sequences were applied to extract soluble organic molecules (SOM) removal of soluble organic molecules
#2 before layer formation 2022-01-01 chemical HCl 6N was used to remove carbonates, sulfides (pyrrhotite and pentlandite) and other minerals, as one step of 2 h, followed by ultrapure water rinsing and a second step overnight. removal of minerals
#3 before layer formation 2022-01-01 chemical A similar sequence with HF(48%):HCl(37%) (2/1 v/v) was run, followed by a short HCl 6N sequence (2 h), to remove any cations that might subsequently react with F- to form insoluble fluorides. removal of cations
#4 before layer formation 2022-01-01 chemical The sample was rinsed again with ultrapure water and CH3OH:CH3Cl (2/1 v/v), for removing encaged free molecules. removing of free molecules
#5 before layer formation 2022-01-01 thermal After having purged the remaining reagents, the sample holder was dismounted and the filter was dried. removal of reagents and water => dried IOM
#6 during layer formation 2022-01-01 mechanical Grains pressed between two diamond windows IOM grains crushed down to a thickness of about 10 microns