Experiment
Title
Ni K edge XAS fluorescence of square planar Nickel(II) with Ni-N2S2 or Ni-S4 coordination at 16K
DOI
10.26302/SSHADE/EXPERIMENT_GV_20160403_001
Data reference
Veronesi, Giulia; Cavazza, Christine; Proux, Olivier (2016): Ni K edge XAS fluorescence of square planar Nickel(II) with Ni-N2S2 or Ni-S4 coordination at 16K. SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_GV_20160403_001
Publications
Type(s)
laboratory measurement
Variable(s)
sample composition
Number of spectra
2
Instrument
X-ray Absorption Spectroscopy measured in fluorescence mode
Sample holder
Oxford-ILL orange cryostat
Standard medium
unknown
Observation mode
spectrum
Spectral range type(s)
hard X
Valid spectral range(s)
Min - Max ($eV$) Sampling ($eV$) Resolution ($eV$) Position accuracy ($eV$) Absorption edge
#1 8099.0 - 9302.0 0.427 $Ni$ (K: 8.3328 $keV$)
Comments
The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Ni metallic foil (first maximum of the derivative set at 8333 eV).
Observation geometry
directional
Observation mode
fixed angles
Comments
Emitted x-rays are collected in a solid angle directed at 90 degrees from the incident beam.
Observation mode
averaged
Variable type(s)
  • sample composition
Date begin
2016-04-03

Versions

Release date
2019-11-19 12:34:23 UTC+0000
Version (Date)
#1 (2019-11-19 12:32:37 UTC+0000, Updated: 2019-11-22 07:41:50 UTC+0000)