- Database
- Experimentalists
- Date
- 2015-01-02
- Provider
- CML laboratory
- Thickness
- 0.5 $\pm$ 0.01 $cm$
- Diameter
- 0.5 $cm$
- Sample changes
- Sample lost further part of structural OH groups in chlorite
- Substrate comments
- High temperature cell of Prying Mantis (TM) DRIFT accessory with cup with KBr windows. The cell was purged with dry (purity 5.0) nitrogen gas at 0.4 l/min rate
- Comments
- Mixture of chlorite and diamond powder in the cup of the high temperature holder of Prying Mantis (TM) DRIFT accessory equiped with cup with KBr windows
- Temperature
- 600.0 $\pm$ 10.0 $^{\circ}C$
- Time at T
- 30.0 $\pm$ 3.0 $min$
- Temperature max
- 600.0 $\pm$ 10.0 $^{\circ}C$
- Comments
- Sample kept under room temperature and pressure
- Type
- molecular gas
- Fluids
-
- N2 5.0 AirProducts 100.0 $\pm$ 0.001 %
- Fluid temperature
- 25.0 $\pm$ 3.0 $^{\circ}C$
- Fluid pressure
- 1013.0 $\pm$ 15.0 $hPa$
- Time at T, P, pH
- 20.0 $\pm$ 3.0 $min$
- Comments
- Fluid type: nitrogen (purity 5.0)
- Number
- 1
- Layers
- Title
- Homogenisation by manual mixing in an agate mortar
- Matters
- Sample
- SG7 chlorite mixed with diamond powder (15% chlorite) at 25°C (this sample)
- Processing steps
-
Step Chronology Date Type Process Changes #1 during layer formation 2015-01-02 mixing Mechanical mixing of chlorite sample with diamond powder in an agate mortar at room P, t for 3 min Formation of homogenous layer consiting of 85% diamond powder and 15% chlorite