Experiment
Title
Magnetite: Vis-NIR-MIR diffuse reflectance and Raman spectra
DOI
10.26302/SSHADE/EXPERIMENT_BS_20250903_001
Data reference
Schmitt, Bernard (2021): Magnetite: Vis-NIR-MIR diffuse reflectance and Raman spectra. SSHADE/DRIMS (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_BS_20250903_001
Database(s)
Experimentalists
Type(s)
laboratory measurement
Description
Magnetite: Visible Near-IR and MIR bidirectional diffuse reflectance, and micro-Raman Far & Mid-IR spectra of powders and crystals
Number of spectra
5
Variable type(s)
  • spectrum type
  • spectral range
Instrument
SHINE Spectro-Gonio bidirectional reflection Vis-NIR
Sample holder
cylindrical raw aluminium sample holders of various sizes for powders
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
Vis, NIR
Valid spectral range(s)
Min - Max ($nm$) Sampling ($nm$) Resolution ($nm$) Position accuracy ($nm$) Absorption edge
#1 400.0 - 678.0 4.0 1.92 0.5
#2 682.0 - 1598.0 4.0 3.8 0.5
#3 1602.0 - 2834.0 4.0 7.65 0.8
#4 2842.0 - 4180.0 8.0 15.45 1.6
Filters
Type Center/Edge ($nm$) Width ($nm$) Place
#1 several high frequency filters output of monochromator
Comments
slit 600µm, resolution vary by up to $\pm2.5%$ over each spectral range
Observation geometry
bidirectional
Observation mode
fixed angles
Incidence angle
0.0°
Emergence angle
30.0°
Azimuth angle
0.0°
Phase angle
30.0°
Resolution illumination
5.8°
Resolution observation
4.1°
Illumination
Observation
Comments
some wavelength dependent polarization
Observation mode
single spot
Spatial resolution
7.5 ${\pm}$ 0.2 $mm$
Comments
illumination with 9 fiber optic spots within 7.5 mm diameter, observation within an ellipse of 23x20 mm
Instrument
Brucker Vertex 70 #2 – reflection Mid-IR
Sample holder
cylindrical raw aluminium sample holders of various sizes for powders
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
MIR
Valid spectral range(s)
Min - Max ($cm^{-1}$) Sampling ($cm^{-1}$) Resolution ($cm^{-1}$) Position accuracy ($cm^{-1}$) Absorption edge
#1 510.0 - 6000.0 0.482 0.96 0.2
Observation geometry
biconical
Observation mode
fixed angles
Incidence angle
0.0°
Emergence angle
30.0°
Azimuth angle
0.0°
Phase angle
30.0°
Illumination
Observation
Comments
some wavelength dependent polarization
Observation mode
single spot
Spatial resolution
4.0 ${\pm}$ 0.2 $mm$
Instrument
Micro-Raman LabRam Soleil - 532 nm
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
MIR, FIR
Valid spectral range(s)
Min - Max ($cm^{-1}$) Sampling ($cm^{-1}$) Resolution ($cm^{-1}$) Position accuracy ($cm^{-1}$) Absorption edge
#1 50.0 - 1840.0 1.85 3.7 0.4
Filters
Type Center/Edge ($cm^{-1}$) Width ($cm^{-1}$) Place
#1 532.3 nm Edge filter 100.0
Comments
diffraction grating: 1200 l/mm - sampling varies from 2.07 to 1.63 $cm^{-1}$ in the 50-1840 $cm^{-1}$ range. Edge filter: 532.3 nm
Observation geometry
confocal
Observation mode
fixed angles
Incidence angle
0.0°
Emergence angle
0.0°
Observation mode
single spot
Objective type
x50 ELWD
Spatial resolution
2.0 ${\mu}m$
Comments
spot of 2 µm in diameter
Date begin - end
2021-04-27 - 2025-09-17

Versions

Release date
2025-10-19 19:02:27+0000 UTC
Version (Date)
#1 (2025-10-19 19:02:27+0000 UTC, Updated: 2025-10-19 19:02:27+0000 UTC)
Sponsors
  • Observatoire des Sciences de l'Univers (OSUG) (SNO SSHADE)