Experiment
                
                Near-infrared reflectance spectra at low temperature (110-290K) of delta, gamma and beta Diammonium hydrogen phosphate [(NH4)2HPO4] powders with three grain size ranges (32-80, 80-125 and 125-150µm)
            
        
        
                            
                                
                            
                            
                                Sub-Experiment
                            
                           32-80 µm grain sizes
                        
                    
                    
                    
                                    
                                        
                                    
                                    
                                        Sub-Experiment
                                    
                                    Phase delta: 110-160K
                                
                            
                            
                                    
                                        
                                            
                                            
                                                
                                                    Spectrum
                                                
                                                
                                                Near-infrared reflectance spectra at 110K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 120K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 130K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 140K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 150K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 160K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                
                            
                                    
                                        
                                    
                                    
                                        Sub-Experiment
                                    
                                    Phase delta-gamma transition: 170-173K
                                
                            
                            
                                    
                                        
                                            
                                            
                                                
                                                    Spectrum
                                                
                                                
                                                Near-infrared reflectance spectra at 170K of the transition between Diammonium hydrogen phosphate-beta and gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 171K of the transition between Diammonium hydrogen phosphate-beta and gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 172K of the transition between Diammonium hydrogen phosphate-beta and gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 173K of the transition between Diammonium hydrogen phosphate-beta and gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                
                            
                                    
                                        
                                    
                                    
                                        Sub-Experiment
                                    
                                    Phase gamma: 174-245K
                                
                            
                            
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 174K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 175K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 176K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 177K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 180K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 190K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 200K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 210K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 220K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 230K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 243K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 244K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 245K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                
                            
                                    
                                        
                                    
                                    
                                        Sub-Experiment
                                    
                                    Phase beta 246-290K
                                
                            
                            
                                    
                                        
                                            
                                            
                                                
                                                    Spectrum
                                                
                                                
                                                Near-infrared reflectance spectra at 246K of Diammonium hydrogen phosphate-delta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 247K of Diammonium hydrogen phosphate-delta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 248K of Diammonium hydrogen phosphate-delta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 249K of Diammonium hydrogen phosphate-delta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 270K of Diammonium hydrogen phosphate-delta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 290K of Diammonium hydrogen phosphate-delta [(NH4)2HPO4] powder with 32-80µm grain size
                                            
                                        
                                    
                                
                            
                            
                                
                            
                            
                                Sub-Experiment
                            
                           80-125 µm grain sizes (300K)
                        
                    
                    
                    
                                    
                                        
                                    
                                    
                                        Sub-Experiment
                                    
                                    Phase delta: 110-160K
                                
                            
                            
                                    
                                        
                                            
                                            
                                                
                                                    Spectrum
                                                
                                                
                                                Near-infrared reflectance spectra at 110K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 80-125µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 120K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 80-125µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 130K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 80-125µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 140K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 80-125µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 150K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 80-125µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 160K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 80-125µm grain size
                                            
                                        
                                    
                                
                            
                                    
                                        
                                    
                                    
                                        Sub-Experiment
                                    
                                    Phase gamma: 180-220K
                                
                            
                            
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 180K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 80-125µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 190K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 80-125µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 200K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 80-125µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 210K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 80-125µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 220K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 80-125µm grain size
                                            
                                        
                                    
                                
                            
                            
                                
                            
                            
                                Sub-Experiment
                            
                           125-150 µm grain sizes (300K)
                        
                    
                    
                    
                                    
                                        
                                    
                                    
                                        Sub-Experiment
                                    
                                    Phase delta: 110-160K
                                
                            
                            
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 110K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 125-150µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 120K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 125-150µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 130K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 125-150µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 140K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 125-150µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 150K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 125-150µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 160K of Diammonium hydrogen phosphate-beta [(NH4)2HPO4] powder with 125-150µm grain size
                                            
                                        
                                    
                                
                            
                                    
                                        
                                    
                                    
                                        Sub-Experiment
                                    
                                    Phase gamma: 180-220K
                                
                            
                            
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 180K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 125-150µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 190K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 125-150µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 200K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 125-150µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 210K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 125-150µm grain size
                                            
                                        
                                    
                                        
                                            
                                            
                                                
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                                                Near-infrared reflectance spectra at 220K of Diammonium hydrogen phosphate-gamma [(NH4)2HPO4] powder with 125-150µm grain size