Sample
Name
thin film H2O ice (initially amorphous and partially cristalized through heating from 50 K to 160 K)
Date
2024-04-08
Thickness
129.0 $\pm$ 0.2 $nm$
Diameter
13000000.0 $nm$
Substrate material
ZnSe
Substrate comments
disk diameter 13 mm, thickness 2 mm
Comments
prepared with the IGLIAS setup - sample deposited at 50 K and then progressively heated up to 160 K. Spectra recorded every additional 10K
Temperature
50.0 $\pm$ 1.0 $K$
Time at T
30.0 $\pm$ 5.0 $min$
Temperature max
50.0 $K$
Type
vacuum
Fluid pressure
2.0e-07 $\pm$ 1.0e-08 $mbar$
Number
1
Layers
Title
condensation of amorphous H2O ice

Precursors

Matters

Produced sample

Sample
thin film H2O ice (initially amorphous and partially cristalized through heating from 50 K to 160 K) (this sample)
Processing steps
Step Chronology Date Type Process Changes
#1 before layer formation 2024-04-08 fluid physical three freeze-thaw cycles with liquid nitrogen to purify the water
#2 before layer formation 2024-04-08 fluid physical sublimation of solid H2O at a few tens of °C under vacuum from solid to gas phase
#3 during layer formation 2024-04-08 layer formation flux of H2O gas was deposited at 50 K under vacuum from gas to solid amorphous ice phase