Sample
Name
LAP04516 KBr Pellet
Date
2021-01-01
Provider
IPAG
Thickness
0.8 $\pm$ 0.1 $mm$
Diameter
13.0 $mm$
Mass
0.301 $\pm$ 0.0015 $g$
Substrate material
sample holder in aluminum with a centered hole to hold the sample
Comments
KBr pellet of 13mm of diameter and 0.8mm thick
Temperature
22.0 $\pm$ 2.0 $^{\circ}C$
Temperature max
22.0 $\pm$ 2.0 $^{\circ}C$
Type
vacuum
Fluid pressure
0.001 $mbar$
Comments
stored in a desiccator
Number
1
Layers
Title
Grinding of the LAP04516 matter, leaching, mixing with KBr, pellet making

Precursors

Matters

Produced sample

Sample
LAP04516 KBr Pellet
Processing steps
Step Chronology Date Type Process Changes
#1 before layer formation 2021-01-01 mechanical grinding bulk meteorite (20-30 mg) reduced to grains with size lower than 10 microns
#2 before layer formation 2021-01-01 chemical chemical leaching to remove minerals related to terrestrial weathering bulk meteorite (10mg) cleaned from terrestrial weathering products - see Krämer Ruggiu et al. (2021) for details on the chemical protocol
#3 before layer formation 2021-01-01 thermal 300 mg of commercial ultrapure KBr powder was heated under ambient air to 80°C overnight (~10h) removal of adsorbed/hydration water in KBr powder
#4 before layer formation 2021-01-01 mixing homogeneous mixing 1.0 mg of grinded and leached meteorite was weighed and mixed with 300 mg of dried commercial ultrapure KBr powder
#5 during layer formation 2021-01-01 pressure pressure formation of a pellet of 13mm diameter and 0.8 mm thick under 400 bars of pressure