Spectrum

Zn K edge XAS HERFD of ZnCys3His peptide at 10K

Title
Zn K edge XAS HERFD of ZnCys3His peptide at 10K
DOI
10.26302/SSHADE/EXPERIMENT_ST_20180418_001
Data reference
Thomas, Sara; Mishra, Bhoopesh (2018): Zn K edge XAS HERFD of Zn compounds at 10K for coordination determination in complex biological systems. SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_ST_20180418_001
Publications
Experiment type
laboratory measurement
Type
fluorescence emission
Intensity unit
AU
Instrument
High Energy Resolution Fluorescence Detection X-ray Absorption Spectroscopy
Sample holder
ESRF helium mini-cryostat
Standard medium
unknown
Observation mode
spectrum
Spectral range type(s)
hard X
Excitation wavelength
hard X
Valid spectral range(s)
Min - Max ($eV$) Sampling ($eV$) Resolution ($eV$) Position accuracy ($eV$) Absorption edge
#1 9512.0 - 10402.0 0.495 $Zn$ (K: 9.6586 $keV$)
Comments
The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Zn metallic foil (first maximum of the derivative set at 9659 eV). The resolution of the spectrometer analyser was 1.4 eV (FWHM of the elastic peak).
Observation geometry
directional
Observation mode
fixed angles
Comments
Emitted x-rays are collected in a solid angle directed at 90 degrees from the incident beam.
Observation mode
averaged
Experiment
Zn K edge XAS HERFD of Zn compounds at 10K for coordination determination in complex biological systems
Date begin
2018-04-19
Release date
2019-09-02 09:17:01 UTC+0000
Version (Date)
#1 (2019-09-02 09:17:01 UTC+0000, Updated: 2023-08-21 15:34:53 UTC+0000)
History
Date Mode Version Status Comments
2019-09-02 09:00:13 UTC+0000 first import #1 valid version
Analysis
raw averaged spectra