Spectrum

Vis-NIR bidirectional reflection spectrum of ammonium carbamate (17 wt%) mixed with pyrrhotite sub-micrometer size grains in a sublimate residue at 173 K

Title
Vis-NIR bidirectional reflection spectrum of ammonium carbamate (17 wt%) mixed with pyrrhotite sub-micrometer size grains in a sublimate residue at 173 K
DOI
10.26302/SSHADE/EXPERIMENT_OP_20191119_001
Data reference
Poch, Olivier; Istiqomah, Istiqomah (2018): Vis-NIR bidirectional reflection spectra of several ammonium salts mixed with pyrrhotite grains in sublimate residues at 173 K. SSHADE/GhoSST (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_OP_20191119_001
Publications
Experiment type
laboratory measurement
Type
reflectance factor
Comments
This spectrum is the average of 5 individual spectra. At 1.3-1.5 µm, 1.8-2.0 µm and 2.4-3.0 µm, the spectrum was affected by strong measurement artifacts due to the presence of water vapor in the optical path, so these wavelength ranges have been removed from the data.
Instrument
SHINE Spectro-Gonio bidirectional reflection Vis-NIR
Sample holder
Aluminum sample holder, cylindrical 48 mm diameter and 5 mm depth closed by a sapphire window and cooled by a He cryostat in a vacuum chamber (Carbo-NIR)
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
Vis, NIR
Valid spectral range(s)
Min - Max ($nm$) Sampling ($nm$) Resolution ($nm$) Position accuracy ($nm$) Absorption edge
#1 700.0 - 1280.0 20.0 10.0
#2 1640.0 - 1640.0 19.0
#3 2040.0 - 2240.0 20.0 19.0
#4 2920.0 - 2980.0 20.0 19.0
#5 3000.0 - 4120.0 20.0 39.0
Filters
Type Center/Edge ($nm$) Width ($nm$) Place
#1 long-pass filters of the spectro-gonio radiometer
Scan number
5
Observation geometry
bidirectional
Observation mode
fixed angles
Incidence angle
0.0°
Emergence angle
30.0°
Azimuth angle
0.0°
Phase angle
30.0°
Resolution observation
4.1°
Comments
The spectro-radio-goniometer SHINE was used in Gognito mode, as described in Potin et al. (2018, https://doi.org/10.1364/AO.57.008279), section D.2. The illumination beam was focused on an area of 6 mm in diameter on the sample, in order to increase the signal-to-noise ratio of our measurements.
Illumination
Observation
Comments
partial polarization variable with wavelength (from monochromator grating)
Observation mode
single spot
Resolutions
6.0 $mm$
Experiment
Vis-NIR bidirectional reflection spectra of several ammonium salts mixed with pyrrhotite grains in sublimate residues at 173 K
Date begin
2018-12-14 17:21:00
Date end
2018-12-17 12:53:00
Release date
2020-02-12 11:12:53 UTC+0000
Version (Date)
#1 (2020-02-12 11:12:53 UTC+0000, Updated: 2020-03-18 09:01:47 UTC+0000)
History
Date Mode Version Status Comments
2019-11-21 09:28:14 UTC+0000 first import #1 valid version new reflectance spectrum
Analysis
raw bidirectional reflectance spectrum calibrated: 1) with "Spectralon 99%" measured under same geometry using its absolute BRDF (0.7-2.1 µm) and 2) with "Infragold" using its relative spectral reflectance (2.1-4.12 µm).
Quality flag
4
Validator(s)