Spectrum

Optical constants of cellulose pyrolyzed at 800°C from UV to FIR

Title
Optical constants of cellulose pyrolyzed at 800°C from UV to FIR
DOI
10.26302/SSHADE/EXPERIMENT_HM_20170912_101
Data reference
Jäger, Cornelia; Mutschke, Harald; Henning, Thomas (1997): Optical constants from UV to FIR for cellulose pyrolized between 400 and 1000°C. SSHADE/DOCCD (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_HM_20170912_101
Publications
Experiment type
laboratory measurement
Type
optical constants
Comments
The spectrum was resampled between 0.2 and 562 µm on a logarithmic wavelength scale
Instrument
Lambda 19 – reflection UV
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
UV
Valid spectral range(s)
Min - Max (μm) Sampling (μm) Resolution (μm) Position accuracy (μm) Absorption edge
#1 0.2 - 0.319 0.001
Scan number
1
Observation geometry
specular
Observation mode
fixed angles
Incidence angle
12.0°
Emergence angle
12.0°
Azimuth angle
180.0°
Phase angle
24.0°
Resolution illumination
6.0°
Resolution observation
6.0°
Illumination
Type of polarization
no
Observation
Type of polarization
no
Observation mode
single spot
Resolutions
5.0 None
Instrument
Lambda 19 – reflection vis
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
Vis
Valid spectral range(s)
Min - Max (μm) Sampling (μm) Resolution (μm) Position accuracy (μm) Absorption edge
#1 0.319 - 0.86 0.001
Scan number
1
Observation geometry
specular
Observation mode
fixed angles
Incidence angle
12.0°
Emergence angle
12.0°
Azimuth angle
180.0°
Phase angle
24.0°
Resolution illumination
6.0°
Resolution observation
6.0°
Illumination
Type of polarization
no
Observation
Type of polarization
no
Observation mode
single spot
Resolutions
5.0 None
Instrument
Lambda 19 – reflection NIR
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
NIR
Valid spectral range(s)
Min - Max (μm) Sampling (μm) Resolution (μm) Position accuracy (μm) Absorption edge
#1 0.86 - 3.2
Scan number
1
Observation geometry
specular
Observation mode
fixed angles
Incidence angle
12.0°
Emergence angle
12.0°
Azimuth angle
180.0°
Phase angle
24.0°
Resolution illumination
6.0°
Resolution observation
6.0°
Illumination
Type of polarization
no
Observation
Type of polarization
no
Observation mode
single spot
Resolutions
5.0 None
Instrument
BRUKER 113v – reflection Mid-IR
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
MIR
Valid spectral range(s)
Min - Max (μm) Sampling (μm) Resolution (μm) Position accuracy (μm) Absorption edge
#1 2.0 - 25.0
Scan number
64
Observation geometry
specular
Observation mode
fixed angles
Incidence angle
12.0°
Emergence angle
12.0°
Azimuth angle
180.0°
Phase angle
24.0°
Resolution illumination
6.0°
Resolution observation
6.0°
Illumination
Type of polarization
no
Observation
Type of polarization
no
Observation mode
single spot
Resolutions
5.0 None
Instrument
BRUKER 113v – reflection Far-IR
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
FIR
Valid spectral range(s)
Min - Max (μm) Sampling (μm) Resolution (μm) Position accuracy (μm) Absorption edge
#1 15.0 - 500.0
Scan number
64
Observation geometry
specular
Observation mode
fixed angles
Incidence angle
12.0°
Emergence angle
12.0°
Azimuth angle
180.0°
Phase angle
24.0°
Resolution illumination
6.0°
Resolution observation
6.0°
Illumination
Type of polarization
no
Observation
Type of polarization
no
Observation mode
single spot
Resolutions
5.0 mm
Instrument
BRUKER 113v – transmission Far-IR
Standard medium
vacuum
Observation mode
spectrum
Spectral range type(s)
FIR
Valid spectral range(s)
Min - Max (μm) Sampling (μm) Resolution (μm) Position accuracy (μm) Absorption edge
#1 15.0 - 500.0
Scan number
64
Observation geometry
direct
Observation mode
fixed angles
Resolution illumination
6.0°
Resolution observation
6.0°
Illumination
Type of polarization
no
Observation
Type of polarization
no
Observation mode
single spot
Resolutions
5.0 None
Experiment
Optical constants from UV to FIR for cellulose pyrolized between 400 and 1000°C
Date begin
1997-01-01
Release date
2018-01-31 23:51:01+0000 UTC
Version (Date)
#1 (2018-01-31 23:51:01+0000 UTC, Updated: 2019-08-16 09:21:21+0000 UTC)
History
Date Mode Version Status Comments
2017-11-03 16:24:31+0000 UTC first import #1 valid version first version
Analysis
The optical constants were determined from the reflectance (spectra measured with FTIR and Lambda 19 were merged) by a Lorentzian-oscillator fit.
Quality flag
4