Spectrum

Fe K edge XAS fluorescence of FeSO4 in buffer

Title
Fe K edge XAS fluorescence of FeSO4 in buffer
DOI
10.26302/SSHADE/EXPERIMENT_FS_20201007_002
Data reference
Stellato, Francesco; Morante, Silvia; Proux, Olivier; Consalvi, Valerio (2020): Fe K edge XAS fluorescence of FeSO4 in buffer for the study of the Iron binding site in the mature and C-terminal regions of wild-type and mutant human frataxin.. SSHADE/FAME (OSUG Data Center). Dataset/Spectral Data. https://doi.org/10.26302/SSHADE/EXPERIMENT_FS_20201007_002
Publications
Experiment type
laboratory measurement
Type
fluorescence emission
Intensity unit
AU
Instrument
X-ray Absorption Spectroscopy measured in fluorescence mode
Sample holder
Oxford-ILL orange cryostat
Standard medium
unknown
Observation mode
spectrum
Spectral range type(s)
hard X
Excitation wavelength
hard X
Valid spectral range(s)
Min - Max ($eV$) Sampling ($eV$) Resolution ($eV$) Position accuracy ($eV$) Absorption edge
#1 7005.0 - 7961.0 0.365 $Fe$ (K: 7.112 $keV$)
Comments
The resolution in the above table is the resolution given by the monochromator. The energy was calibrated by measuring the absorption edge of a reference: Fe metallic foil (first maximum of the derivative set at 7112 eV).
Observation geometry
directional
Observation mode
fixed angles
Comments
Emitted x-rays are collected in a solid angle directed at 90 degrees from the incident beam.
Observation mode
averaged
Experiment
Fe K edge XAS fluorescence of FeSO4 in buffer for the study of the Iron binding site in the mature and C-terminal regions of wild-type and mutant human frataxin.
Date begin
2020-10-07
Release date
2022-11-02 11:14:29 UTC+0000
Version (Date)
#1 (2022-11-02 11:14:29 UTC+0000, Updated: 2022-11-02 11:14:29 UTC+0000)
History
Date Mode Version Status Comments
2020-10-29 13:32:17 UTC+0000 first import #1 valid version
Analysis
raw averaged spectra