Sample
Name
Ammonium biphosphate powder (phase PE) - grains: 32-80µm
Date
2020-11-23
Thickness
3.5 $\pm$ 0.1 $mm$
Diameter
14.0 $mm$
Volume
542.6 $mm^3$
Mass
0.397 $\pm$ 0.002 $g$
Surface roughness
smooth
Sample changes
partly transformed back to phase PE of Ammonium biphosphate
Substrate material
Aluminium
Substrate comments
cylindrical hole, diameter: 14 mm, depth: 3.5 mm
Temperature
148.0 $\pm$ 0.5 $K$
Time at T
5.0 $min$
Temperature max
300.0 $\pm$ 3.0 $K$
Comments
recording of the spectrum takes 64 min
Type
purged air
Fluid temperature
148.0 $K$
Fluid pressure
0.47 $bar$
Comments
air is dried by condensation of water at bottom of cooled cell
Number
1
Layers