- Database
- Experimentalists
- Date
- 2020-11-23
- Previous sample
- Ammonium biphosphate powder (phase PE) - grains: 32-80µm
- Parent sample
- Ammonium biphosphate powder (phase PE) - grains: 32-80µm
- Thickness
- 3.5 ± 0.1 mm
- Diameter
- 14.0 mm
- Volume
- 542.6 mm3
- Mass
- 0.397 ± 0.002 g
- Surface roughness
- smooth
- Sample changes
- fully transformed to phase AFE of Ammonium biphosphate
- Substrate material
- Aluminium
- Substrate comments
- cylindrical hole, diameter: 14 mm, depth: 3.5 mm
- Comments
- formed by solid-solid phase transition of a sample of Ammonium biphosphate (phase PE)
- Temperature
- 147.0 ± 0.5 K
- Time at T
- 5.0 min
- Temperature max
- 148.0 ± 1.0 K
- Comments
- recording of the spectrum takes 64 min
- Type
- purged air
- Fluid temperature
- 147.0 K
- Fluid pressure
- 0.5 bar
- Comments
- air is dried by condensation of water at bottom of cooled cell
- Number
- 1
- Layers
-
- Layer #1 , 3.5 mm